| ○種別 (必須): | □ | 学術論文 (審査論文)
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| ○言語 (必須): | □ | 英語
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| ○招待 (推奨): | □ | 依頼
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| ○審査 (推奨): | □ | Peer Review
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| ○カテゴリ (推奨): | □ | 研究
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| ○共著種別 (推奨): | □ | 学内共著 (徳島大学内研究者との共同研究 (学外研究者を含まない))
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| ○学究種別 (推奨): | □ | 博士課程学生による研究報告
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| ○組織 (推奨): | 1. | 徳島大学.薬学研究科 (2004年4月1日〜)
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| ○著者 (必須): | 1. | (英) Kakiuchi Naoya (日) 柿内 直哉 (読) かきうち なおや
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| ○学籍番号 (推奨): | □ | ****
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| 2. | 竹内 政樹 ([徳島大学.大学院医歯薬学研究部.薬学域.薬科学部門.創薬科学系.分析科学])
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| 3. | 田中 秀治 ([徳島大学.大学院医歯薬学研究部.薬学域.薬科学部門.創薬科学系.分析科学]/徳島大学薬学部創製薬科学科分析科学研究室/徳島大学大学院薬科学教育部分析科学分野)
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| ○題名 (必須): | □ | (英) Integrated continuous flow method with dual feedback-based controls for online analysis and process control (日)
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| ○要約 (任意): | □ | (英) The concept of an integrated automated continuous flow method with dual feedback controls is presented for diluting a stock solution to provide a solution of a given concentration. The one control is used for the online process monitoring by a feedback-based flow ratiometry, where the product (the diluted liquid) is titrated through the rapid bidirectional scan of the product/reagent flow ratio. The feedback control limits the scanning to the necessary range to increase the analytical throughput. The other control is used for the process control to output the product with a preset concentration. The merging ratio of the stock solution and a solvent (diluent) is changed based on the information from the online analysis. The concept was verified by applying it to producing 0.1 mol dm CHCOOH. When the stock concentration was changed from 0.1 (reference concentration) to 0.3 and then 0.2 mol dm, the system searched for the suitable merging ratio and converged the output concentration to the reference value within 7.43 min with a relative error below 1.05%. The mean throughput rate of the process analysis was 11.2 titrations min. Successful results were also obtained for the 0.1 mol dm HCl production. The present concept could be the basis for process control with reduced wasteful output and effluent treatment with eco-friendly treated water discharge, resulting in the contribution to SDGs' goals of 6 (Clean water and sanitation), 9 (Industry, innovation and infrastructure), and 14 (Life below water). (日)
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| ○キーワード (推奨): |
| ○発行所 (推奨): | □ | Springer-Verlag.シュプリンガー ジャパン
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| ○誌名 (必須): | □ | Analytical Sciences ([日本分析化学会])
(pISSN: 0910-6340, eISSN: 1348-2246)
| ○ISSN (任意): | □ | 1348-2246
ISSN: 0910-6340
(pISSN: 0910-6340, eISSN: 1348-2246) Title: Analytical sciences : the international journal of the Japan Society for Analytical ChemistryTitle(ISO): Anal SciSupplier: 社団法人 日本分析化学会Publisher: Springer International Publishing AG (NLM Catalog)
(医中誌Web)
(J-STAGE)
(Scopus)
(CrossRef)
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| ○巻 (必須): | □ | 39
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| ○号 (必須): | □ |
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| ○頁 (必須): | □ |
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| ○都市 (任意): |
| ○年月日 (必須): | □ | 西暦 2023年 0月 初日 (令和 5年 0月 初日)
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| ○URL (任意): |
| ○DOI (任意): | □ | 10.1007/s44211-022-00206-3 (→Scopusで検索)
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| ○PMID (任意): | □ | 36273392 (→Scopusで検索)
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| ○指導教員 (推奨): | 1. | 田中 秀治 ([徳島大学.大学院医歯薬学研究部.薬学域.薬科学部門.創薬科学系.分析科学]/徳島大学薬学部創製薬科学科分析科学研究室/徳島大学大学院薬科学教育部分析科学分野)
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| ○備考 (任意): | 1. | (英) Article.ELocationID: 10.1007/s44211-022-00206-3 (日)
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| 2. | (英) Article.PublicationTypeList.PublicationType: Journal Article (日)
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| 3. | (英) KeywordList.Keyword: Feedback control (日)
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| 4. | (英) KeywordList.Keyword: Feedback-based flow ratiometry (日)
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| 5. | (英) KeywordList.Keyword: Flow titration (日)
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| 6. | (英) KeywordList.Keyword: Online analysis (日)
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| 7. | (英) KeywordList.Keyword: Process control (日)
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| 8. | (英) KeywordList.Keyword: SDGs (日)
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